Table of Contents

1 -  AS ISO 15472-2006 Surface chemical analysis - X-ray photoelectron spectrometers - Calibration of energy scales
4 -  PREFACE
5 -  CONTENTS
6 -  INTRODUCTION
7 -  1 Scope
7 -  2 Normative reference
7 -  3 Symbols and abbreviated terms
8 -  4 Outline of method
12 -  5 Procedure for calibrating the energy scale
12 -  5.1 Obtaining the reference samples
12 -  5.2 Mounting the samples
12 -  5.3 Cleaning the samples
12 -  5.4 Choosing the spectrometer settings for which energy calibration is required
12 -  5.5 Operating the instrument
13 -  5.6 Options for initial or subsequent calibration measurements
13 -  5.7 Measurements for the peak binding-energy repeatability standard deviation and the scale linearity
14 -  5.8 Calculating the peak binding-energy repeatability standard deviation
17 -  5.9 Checking the binding-energy scale linearity
18 -  5.10 Procedure for the regular determination of the calibration error
19 -  5.11 Procedures for correction of the instrument binding-energy scale
21 -  5.12 Next calibration
21 -  5.13 Establishing the calibration interval
22 -  Annex A (normative) Least-squares determination of the peak binding energy by a simple computational method
25 -  Annex B (informative) Derivation of uncertainties
27 -  Annex C (informative) Citation of the uncertainties of measured binding energies
29 -  Annex D (informative) Measurements of modified Auger parameters measured using XPS instruments equipped with a monochromated Al X-ray source
32 -  Bibliography

Abstract

Adopts ISO 15472:2001 to specify a method for calibrating the binding-energy scales of X-ray photoelectron spectrometers for general analytical purposes.

General Product Information

Published
Document Type	Standard
Status	Current
Publisher	Standards Australia
ProductNote	Pending Revision indicates that as a result of the Aged Standards review process, the document needs updating. If no project proposal, meeting the quality criteria, is received within the 12 month timeframe, the document shall be withdrawn.
Pages
ISBN
Committee	CH-016
Supersedes	DR 06405 CP