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AS 1038.6.3.2-2003 (R2013)
M00003503
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AS 1038.6.3.2-2003 (R2013)
Coal and coke - Analysis and testing Higher rank coal and coke - Ultimate analysis - Total sulfur - High-temperature combustion method
Standards Australia
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Table of Contents
<toc>
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<pageno>1</pageno>
<text>AS 1038.6.3.2-2003 COAL AND COKE-ANALYSIS AND TESTING - HIGHER RANK COAL AND COKE-ULTIMATE ANALYSIS-TOTAL SULFUR-HIGH...</text>
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<pageno>4</pageno>
<text>PREFACE</text>
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<pageno>5</pageno>
<text>CONTENTS</text>
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<pageno>6</pageno>
<text>FOREWORD</text>
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<bookmark index='4'>
<pageno>7</pageno>
<text>1 SCOPE</text>
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<bookmark index='5'>
<pageno>7</pageno>
<text>2 REFERENCED DOCUMENTS</text>
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<bookmark index='6'>
<pageno>7</pageno>
<text>3 DEFINITIONS</text>
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<pageno>7</pageno>
<text>3.1 Repeatability (r)</text>
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</bookmark>
<bookmark index='8'>
<pageno>7</pageno>
<text>4 PRINCIPLE</text>
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<bookmark index='9'>
<pageno>8</pageno>
<text>5 SAFETY</text>
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<bookmark index='10'>
<pageno>8</pageno>
<text>6 REAGENTS</text>
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<pageno>8</pageno>
<text>6.1 General</text>
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<bookmark index='12'>
<pageno>8</pageno>
<text>6.2 Aluminium oxide</text>
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<bookmark index='13'>
<pageno>8</pageno>
<text>6.3 Alkaline absorbent</text>
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<bookmark index='14'>
<pageno>8</pageno>
<text>6.4 Sodium tetraborate solution (0.025 mol/L)</text>
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<bookmark index='15'>
<pageno>8</pageno>
<text>6.5 Standard sulfuric acid solution (0.0125 mol/L)</text>
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<bookmark index='16'>
<pageno>8</pageno>
<text>6.6 Hydrogen peroxide solution (9 g/L)</text>
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<bookmark index='17'>
<pageno>8</pageno>
<text>6.7 Mercury(II) oxycyanide solution</text>
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<bookmark index='18'>
<pageno>8</pageno>
<text>6.8 Screened indicator solution</text>
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<bookmark index='19'>
<pageno>9</pageno>
<text>6.9 Oxygen</text>
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</bookmark>
<bookmark index='20'>
<pageno>9</pageno>
<text>7 APPARATUS</text>
<bookmark index='21'>
<pageno>9</pageno>
<text>7.1 Purification train</text>
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<bookmark index='22'>
<pageno>9</pageno>
<text>7.2 Heating unit</text>
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<bookmark index='23'>
<pageno>9</pageno>
<text>7.3 Combustion tube</text>
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<bookmark index='24'>
<pageno>9</pageno>
<text>7.4 Combustion boat</text>
</bookmark>
<bookmark index='25'>
<pageno>9</pageno>
<text>7.5 Silica pusher</text>
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<bookmark index='26'>
<pageno>9</pageno>
<text>7.6 Nickel-chromium wire</text>
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<bookmark index='27'>
<pageno>9</pageno>
<text>7.7 Flowmeter</text>
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<bookmark index='28'>
<pageno>9</pageno>
<text>7.8 Pressure gauge</text>
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<bookmark index='29'>
<pageno>10</pageno>
<text>7.9 Silica adaptor</text>
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<bookmark index='30'>
<pageno>10</pageno>
<text>7.10 Absorption vessel</text>
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<bookmark index='31'>
<pageno>10</pageno>
<text>7.11 Heat-resistant stopper or tubing</text>
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<bookmark index='32'>
<pageno>10</pageno>
<text>7.12 Pressure regulator</text>
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<bookmark index='33'>
<pageno>10</pageno>
<text>7.13 Vacuum pump</text>
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<bookmark index='34'>
<pageno>10</pageno>
<text>7.14 Weighing device</text>
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</bookmark>
<bookmark index='35'>
<pageno>10</pageno>
<text>8 SAMPLE</text>
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<bookmark index='36'>
<pageno>10</pageno>
<text>9 PROCEDURE</text>
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<pageno>10</pageno>
<text>9.1 Preparation of apparatus</text>
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<bookmark index='38'>
<pageno>11</pageno>
<text>9.2 Determination of the blank</text>
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<bookmark index='39'>
<pageno>12</pageno>
<text>9.3 Combustion and absorption</text>
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<bookmark index='40'>
<pageno>12</pageno>
<text>9.4 Measurement</text>
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<bookmark index='41'>
<pageno>13</pageno>
<text>10 CALCULATION</text>
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<bookmark index='42'>
<pageno>13</pageno>
<text>11 REPORTING OF RESULTS</text>
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<pageno>13</pageno>
<text>12 PRECISION</text>
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<pageno>13</pageno>
<text>13 TEST REPORT</text>
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</toc>
Abstract
Sets out a method for determining the total sulfur content of an analysis sample by high temperature combustion.
RECONFIRMATION NOTICE
Technical Committee MN-001 has reviewed the content of this publication and in accordance with Standards Australia procedures for reconfirmation, it has been determined that the publication is still valid and does not require change.
Certain documents referenced in the publication may have been amended since the original date of publication. Users are advised to ensure that they are using the latest versions of such documents as appropriate, unless advised otherwise in this Reconfirmation Notice.
Approved for reconfirmation in accordance with Standards Australia procedures for reconfirmation on 15 July 2013.
The following are represented on Technical Committee MN-001:
Australasian Institute of Mining and Metallurgy
Australian Coal Association
Australian Coal Industry Reference Samples
Australian Coal Preparation Society
Bureau of Steel Manufacturers of Australia
Coalfield Geology Council of NSW
CSIRO Energy Technology
National Association of Testing Authorities Australia
National Generators Forum
The University of New South Wales
The University of Queensland
University of Newcastle
To view or download a copy of the reconfirmation notice please go to the reconfirmation link near the top of this page.
Scope
This Standard sets out a method for the determination of total sulfur in the analysis sample of higher rank coal and coke by the high-temperature combustion method.
General Product Information
| Document Type | Standard |
| Status | Current |
| Publisher | Standards Australia |
| ProductNote | Reconfirmed 06-08-2013 |
| Committee | MN-001 |
| Supersedes |
|