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AS 1038.13-1990 (R2013)

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AS 1038.13-1990 (R2013)

Coal and coke - Analysis and testing Tests specific to coke

Standards Australia

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Table of Contents

<toc>
<bookmarktable>
<bookmark index=&apos;0&apos;>
<pageno>1</pageno>
<text>AS 1038.13-1990 METHODS FOR THE ANALYSIS AND TESTING OF COAL AND COKE - TESTS SPECIFIC TO COKE</text>
<bookmark index=&apos;1&apos;>
<pageno>4</pageno>
<text>PREFACE</text>
</bookmark>
<bookmark index=&apos;2&apos;>
<pageno>5</pageno>
<text>CONTENTS</text>
</bookmark>
<bookmark index=&apos;3&apos;>
<pageno>6</pageno>
<text>SECTION 1. SCOPE AND GENERAL</text>
<bookmark index=&apos;4&apos;>
<pageno>6</pageno>
<text>1.1 SCOPE.</text>
</bookmark>
<bookmark index=&apos;5&apos;>
<pageno>6</pageno>
<text>1.2 REFERENCED DOCUMENTS.</text>
</bookmark>
<bookmark index=&apos;6&apos;>
<pageno>6</pageno>
<text>1.3 DEFINITIONS.</text>
<bookmark index=&apos;7&apos;>
<pageno>6</pageno>
<text>1.3.1 Coke</text>
</bookmark>
<bookmark index=&apos;8&apos;>
<pageno>6</pageno>
<text>1.3.2 Micum indices</text>
</bookmark>
<bookmark index=&apos;9&apos;>
<pageno>6</pageno>
<text>1.3.3 IRSID indices</text>
</bookmark>
<bookmark index=&apos;10&apos;>
<pageno>6</pageno>
<text>1.3.4 ASTM coke strength factors</text>
</bookmark>
<bookmark index=&apos;11&apos;>
<pageno>6</pageno>
<text>1.3.5 JIS indices</text>
</bookmark>
<bookmark index=&apos;12&apos;>
<pageno>6</pageno>
<text>1.3.6 Shatter indices</text>
</bookmark>
<bookmark index=&apos;13&apos;>
<pageno>6</pageno>
<text>1.3.7 Coke reactivity index (CRI)</text>
</bookmark>
<bookmark index=&apos;14&apos;>
<pageno>6</pageno>
<text>1.3.8 Coke strength after reduction (CSR) (post-reaction strength)</text>
</bookmark>
</bookmark>
<bookmark index=&apos;15&apos;>
<pageno>6</pageno>
<text>1.4 SAFETY.</text>
</bookmark>
<bookmark index=&apos;16&apos;>
<pageno>6</pageno>
<text>1.5 SAMPLE.</text>
</bookmark>
</bookmark>
<bookmark index=&apos;17&apos;>
<pageno>7</pageno>
<text>SECTION 2. DETERMINATION OF MECHANICAL STRENGTH</text>
<bookmark index=&apos;18&apos;>
<pageno>7</pageno>
<text>2.1 DETERMINATION OF MICUM INDICES.</text>
<bookmark index=&apos;19&apos;>
<pageno>7</pageno>
<text>2.1.1 Introduction.</text>
</bookmark>
<bookmark index=&apos;20&apos;>
<pageno>7</pageno>
<text>2.1.2 Principle.</text>
</bookmark>
<bookmark index=&apos;21&apos;>
<pageno>7</pageno>
<text>2.1.3 Apparatus.</text>
</bookmark>
<bookmark index=&apos;22&apos;>
<pageno>8</pageno>
<text>2.1.4 Test sample.</text>
</bookmark>
<bookmark index=&apos;23&apos;>
<pageno>8</pageno>
<text>2.1.5 Procedure.</text>
</bookmark>
<bookmark index=&apos;24&apos;>
<pageno>8</pageno>
<text>2.1.6 Calculation of results.</text>
</bookmark>
<bookmark index=&apos;25&apos;>
<pageno>8</pageno>
<text>2.1.7 Reporting of results.</text>
</bookmark>
<bookmark index=&apos;26&apos;>
<pageno>9</pageno>
<text>2.1.8 Precision.</text>
</bookmark>
<bookmark index=&apos;27&apos;>
<pageno>9</pageno>
<text>2.1.9 Test report.</text>
</bookmark>
</bookmark>
<bookmark index=&apos;28&apos;>
<pageno>9</pageno>
<text>2.2 DETERMINATION OF IRSID INDICES.</text>
<bookmark index=&apos;29&apos;>
<pageno>9</pageno>
<text>2.2.1 Principle.</text>
</bookmark>
<bookmark index=&apos;30&apos;>
<pageno>9</pageno>
<text>2.2.2 Procedure.</text>
</bookmark>
<bookmark index=&apos;31&apos;>
<pageno>9</pageno>
<text>2.2.3 Calculation of results.</text>
</bookmark>
<bookmark index=&apos;32&apos;>
<pageno>9</pageno>
<text>2.2.4 Reporting of results.</text>
</bookmark>
<bookmark index=&apos;33&apos;>
<pageno>9</pageno>
<text>2.2.5 Precision.</text>
</bookmark>
<bookmark index=&apos;34&apos;>
<pageno>9</pageno>
<text>2.2.6 Test report.</text>
</bookmark>
</bookmark>
<bookmark index=&apos;35&apos;>
<pageno>9</pageno>
<text>2.3 ASTM TUMBLER TEST.</text>
<bookmark index=&apos;36&apos;>
<pageno>9</pageno>
<text>2.3.1 Principle.</text>
</bookmark>
<bookmark index=&apos;37&apos;>
<pageno>9</pageno>
<text>2.3.2 Apparatus.</text>
</bookmark>
<bookmark index=&apos;38&apos;>
<pageno>10</pageno>
<text>2.3.3 Test sample.</text>
</bookmark>
<bookmark index=&apos;39&apos;>
<pageno>10</pageno>
<text>2.3.4 Procedure.</text>
</bookmark>
<bookmark index=&apos;40&apos;>
<pageno>10</pageno>
<text>2.3.5 Calculation of results.</text>
</bookmark>
<bookmark index=&apos;41&apos;>
<pageno>10</pageno>
<text>2.3.6 Reporting of results.</text>
</bookmark>
<bookmark index=&apos;42&apos;>
<pageno>10</pageno>
<text>2.3.7 Precision.</text>
</bookmark>
<bookmark index=&apos;43&apos;>
<pageno>10</pageno>
<text>2.3.8 Test report.</text>
</bookmark>
</bookmark>
<bookmark index=&apos;44&apos;>
<pageno>10</pageno>
<text>2.4 JIS DRUM TEST.</text>
<bookmark index=&apos;45&apos;>
<pageno>10</pageno>
<text>2.4.1 Principle.</text>
</bookmark>
<bookmark index=&apos;46&apos;>
<pageno>10</pageno>
<text>2.4.2 Method A.</text>
</bookmark>
<bookmark index=&apos;47&apos;>
<pageno>12</pageno>
<text>2.4.3 Method B.</text>
</bookmark>
<bookmark index=&apos;48&apos;>
<pageno>12</pageno>
<text>2.4.4 Reporting of results.</text>
</bookmark>
<bookmark index=&apos;49&apos;>
<pageno>12</pageno>
<text>2.4.5 Precision.</text>
</bookmark>
<bookmark index=&apos;50&apos;>
<pageno>12</pageno>
<text>2.4.6 Test report.</text>
</bookmark>
</bookmark>
<bookmark index=&apos;51&apos;>
<pageno>13</pageno>
<text>2.5 SHATTER TEST.</text>
<bookmark index=&apos;52&apos;>
<pageno>13</pageno>
<text>2.5.1 Principle.</text>
</bookmark>
<bookmark index=&apos;53&apos;>
<pageno>13</pageno>
<text>2.5.2 Apparatus.</text>
</bookmark>
<bookmark index=&apos;54&apos;>
<pageno>14</pageno>
<text>2.5.3 Method A.</text>
</bookmark>
<bookmark index=&apos;55&apos;>
<pageno>14</pageno>
<text>2.5.4 Method B.</text>
</bookmark>
<bookmark index=&apos;56&apos;>
<pageno>15</pageno>
<text>2.5.5 Calculation of results.</text>
</bookmark>
<bookmark index=&apos;57&apos;>
<pageno>15</pageno>
<text>2.5.6 Reporting of results.</text>
</bookmark>
<bookmark index=&apos;58&apos;>
<pageno>15</pageno>
<text>2.5.7 Precision.</text>
</bookmark>
<bookmark index=&apos;59&apos;>
<pageno>15</pageno>
<text>2.5.8 Test report.</text>
</bookmark>
</bookmark>
</bookmark>
<bookmark index=&apos;60&apos;>
<pageno>17</pageno>
<text>SECTION 3. DETERMINATION OF COKE REACTIVITY INDEX AND COKE STRENGTH AFTER REACTION</text>
<bookmark index=&apos;61&apos;>
<pageno>17</pageno>
<text>3.1 PRINCIPLE.</text>
</bookmark>
<bookmark index=&apos;62&apos;>
<pageno>17</pageno>
<text>3.2 REAGENTS.</text>
<bookmark index=&apos;63&apos;>
<pageno>17</pageno>
<text>3.2.1 Nitrogen</text>
</bookmark>
<bookmark index=&apos;64&apos;>
<pageno>17</pageno>
<text>3.2.2 Carbon dioxide</text>
</bookmark>
</bookmark>
<bookmark index=&apos;65&apos;>
<pageno>17</pageno>
<text>3.3 APPARATUS.</text>
<bookmark index=&apos;66&apos;>
<pageno>17</pageno>
<text>3.3.1 Electric furnace (see Figure 3.1)</text>
</bookmark>
<bookmark index=&apos;67&apos;>
<pageno>17</pageno>
<text>3.3.2 Reaction vessel</text>
</bookmark>
<bookmark index=&apos;68&apos;>
<pageno>17</pageno>
<text>3.3.3 Test thermocouple</text>
</bookmark>
<bookmark index=&apos;69&apos;>
<pageno>17</pageno>
<text>3.3.4 External control thermocouple</text>
</bookmark>
<bookmark index=&apos;70&apos;>
<pageno>17</pageno>
<text>3.3.5 Gas flow meters</text>
</bookmark>
<bookmark index=&apos;71&apos;>
<pageno>17</pageno>
<text>3.3.6 Strength tumbler</text>
</bookmark>
<bookmark index=&apos;72&apos;>
<pageno>17</pageno>
<text>3.3.7 Sieves</text>
</bookmark>
<bookmark index=&apos;73&apos;>
<pageno>17</pageno>
<text>3.3.8 Magnet</text>
</bookmark>
<bookmark index=&apos;74&apos;>
<pageno>17</pageno>
<text>3.3.9 Balance</text>
</bookmark>
</bookmark>
<bookmark index=&apos;75&apos;>
<pageno>17</pageno>
<text>3.4 TEST SAMPLE.</text>
</bookmark>
<bookmark index=&apos;76&apos;>
<pageno>17</pageno>
<text>3.5 PROCEDURE.</text>
</bookmark>
<bookmark index=&apos;77&apos;>
<pageno>17</pageno>
<text>3.6 CALCULATION OF RESULTS.</text>
</bookmark>
<bookmark index=&apos;78&apos;>
<pageno>17</pageno>
<text>3.7 REPORTING OF RESULTS.</text>
</bookmark>
<bookmark index=&apos;79&apos;>
<pageno>18</pageno>
<text>3.8 PRECISION.</text>
</bookmark>
<bookmark index=&apos;80&apos;>
<pageno>18</pageno>
<text>3.9 TEST REPORT.</text>
</bookmark>
</bookmark>
<bookmark index=&apos;81&apos;>
<pageno>22</pageno>
<text>APPENDIX A - NOTES ON MICUM TEST</text>
<bookmark index=&apos;82&apos;>
<pageno>22</pageno>
<text>A1 STABILIZATION OF COKE BEFORE DETERMINATION OF MICUM INDICES</text>
</bookmark>
<bookmark index=&apos;83&apos;>
<pageno>22</pageno>
<text>A2 EXTENDED MICUM TEST.</text>
</bookmark>
</bookmark>
</bookmark>
</bookmarktable>
</toc>

Abstract

Sets out procedures for the determination of properties which are specific for coke, covering mechanical strength, reactivity and post-reaction strength.

RECONFIRMATION NOTICE
Technical Committee MN-001 has reviewed the content of this publication and in accordance with Standards Australia procedures for reconfirmation, it has been determined that the publication is still valid and does not require change.
Certain documents referenced in the publication may have been amended since the original date of publication. Users are advised to ensure that they are using the latest versions of such documents as appropriate, unless advised otherwise in this Reconfirmation Notice.
Approved for reconfirmation in accordance with Standards Australia procedures for reconfirmation on 15 July 2013.
The following are represented on Technical Committee MN-001:

Australasian Institute of Mining and Metallurgy
Australian Coal Association
Australian Coal Industry Reference Samples
Australian Coal Preparation Society
Bureau of Steel Manufacturers of Australia
Coalfield Geology Council of NSW
CSIRO Energy Technology
National Association of Testing Authorities Australia
National Generators Forum
The University of New South Wales
The University of Queensland
University of Newcastle


To view or download a copy of the reconfirmation notice please go to the reconfirmation link near the top of this page.

Scope

This Standard sets out procedures for the determination of properties which are specific to coke. The various Sections cover the determination of mechanical strength, reactivity and post-reaction strength.

General Product Information

Document Type Standard
Status Current
Publisher Standards Australia
ProductNote Reconfirmed 06-08-2013
Committee MN-001
Under Revision
  • DR 06165 CP
Supersedes
  • DR 88139