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BS EN 14526 : 2017

M00020750

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BS EN 14526 : 2017

FOODSTUFFS - DETERMINATION OF SAXITOXIN-GROUP TOXINS IN SHELLFISH - HPLC METHOD USING PRE-COLUMN DERIVATIZATION WITH PEROXIDE OR PERIODATE OXIDATION

British Standards Institution

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Table of Contents

European foreword <br>Introduction <br>1 Scope <br>2 Normative references <br>3 Principle <br>4 Reagents <br>5 Apparatus <br>6 Procedure<br>7 HPLC determination <br>8 Calibration curve <br>9 Identification <br>10 Calculation <br>11 Precision <br>12 Test report <br>Annex A (informative) - Precision data <br>Bibliography

Abstract

Defines a method for the quantitative determination of saxitoxin (STX), decarbamoyl saxitoxin (dcSTX), neosaxitoxin (NEO), decarbamoyl neosaxitoxin (dcNEO), gonyautoxin 1 and 4 (GTX1,4; sum of isomers), gonyautoxin 2 and 3 (GTX2,3; sum of isomers), gonyautoxin 5 (GTX5 also called B1), gonyautoxin 6 (GTX6 also called B2), decarbamoyl gonyautoxin 2 and 3 (dcGTX2,3; sum of isomers), N-sulfocarbamoyl-gonyautoxin 1 and 2 (C1,2; sum of isomers) and (depending on the availability of certified reference materials (CRMs)) N-sulfocarbamoyl-gonyautoxin 3 and 4 (C3,4; sum of isomers) in (raw) mussels, oysters, scallops and clams.

General Product Information

Document Type Standard
Status Current
Publisher British Standards Institution
Committee AW/275
Supersedes
  • 15/30317860 DC : 0
  • 02/710011 DC : DRAFT AUG 2002