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BS EN ISO 18635 : 2016

M00014963

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BS EN ISO 18635 : 2016

WATER QUALITY - DETERMINATION OF SHORT-CHAIN POLYCHLORINATED ALKANES (SCCPS) IN SEDIMENT, SEWAGE SLUDGE AND SUSPENDED (PARTICULATE) MATTER - METHOD USING GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC-MS) AND ELECTRON CAPTURE NEGATIVE IONIZATION (ECNI)

British Standards Institution

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Table of Contents

Foreword<br>Introduction<br>1 Scope<br>2 Normative references<br>3 Principle<br>4 Interferences<br>5 Reagents<br>6 Apparatus<br>7 Sampling and sample pretreatment<br>8 Procedure<br>9 Expression of results<br>10 Test report<br>Annex A (normative) - Programme for pressurized liquid<br>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;extraction<br>Annex B (informative) - Explanation of the calibration of the<br>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;sum of SCCPs with multiple linear regression<br>Annex C (informative) - Examples of typical GC-MS conditions<br>Annex D (normative) - Alternative clean-up with column<br>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;chromatography<br>Annex E (informative) - Alternative clean-up with gel<br>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;chromatography<br>Annex F (informative) - Typical chromatograms of standard<br>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;solutions 1 [MU]g/ml<br>Annex G (informative) - Presentation of goodness of fit of<br>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;the calibration<br>Annex H (informative) - Example for recoveries of<br>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;quality assurance solutions<br>Annex I (informative) - Chromatograms of real samples<br>Annex J (informative) - Performance data<br>Annex K (informative) - Quality control check solutions<br>Bibliography

Abstract

Defines a method for the quantitative determination of the sum of short-chain polychlorinated n-alkanes also known as short-chain polychlorinated paraffins (SCCPs) in the carbon bond range n-C[10] to n-[C13] inclusive, in mixtures with chlorine mass fractions ('contents') between 50% and 67%, including approximately 6000 of approximately 8000 congeners.

General Product Information

Document Type Standard
Status Current
Publisher British Standards Institution
Committee EH/3/2
Supersedes
  • 14/30280237 DC : 0