M00029292
New product
WORKPLACE ATMOSPHERES - DETERMINATION OF TOTAL ISOCYANATE GROUPS IN AIR USING 1-(9-ANTHRACENYLMETHYL)PIPERAZINE (MAP) REAGENT AND LIQUID CHROMATOGRAPHY
International Organization for Standardization
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Availability date: 11/05/2021
Foreword
Introduction
1 Scope
2 Normative references
3 Principle
4 Reagents and materials
5 Apparatus
6 Air sampling
6.1 Pre-sampling laboratory preparation
6.2 Pre-sampling field preparation
6.3 Collection of air samples
6.4 Blanks and negative controls
6.5 Bulk products
6.6 Shipment of samples
6.7 Filter test samples
6.8 Impinger test samples
7 HPLC analysis
7.1 Instrumental settings
7.2 HPLC programme
8 Data handling
8.1 Monomer measurement
8.2 Oligomer measurement (total detectable isocyanate)
9 Calibration and quality control
9.1 Standard matching solutions
9.2 Calibration curves
9.3 Blank tests
9.4 Bulk products
9.5 Quality control spikes
10 Calculations
10.1 Monomer
10.2 Oligomers (total detectable isocyanate)
11 Interferences
12 Determination of performance characteristics
12.1 Introduction
12.2 Assessment of performance characteristics
Annex A (informative) Performance characteristics
Bibliography
Provides general guidance for the sampling and analysis of airborne organic isocyanates in workplace air.
Published | |
Document Type | Standard |
Status | Current |
Publisher | International Organization for Standardization |
Pages | |
ISBN | |
Committee | TC 146 |