Table of Contents

1 Scope
2 Normative references
3 General
4 Object substances and classification of analysis methods
5 Sampling methods
5.1 Sampling methods for cadmium, lead, nickel, manganese,
vanadium, chromium, beryllium, arsenic and selenium
5.2 Sampling method for gaseous compound such as arsenic
hydride, hydrogen selenide or others
6 Preparation of sample solution
6.1 Sample solution preparation of cadmium, lead, nickel,
manganese, and vanadium
6.2 Preparation of chromium sample solution
6.3 Preparation of beryllium sample solution
6.4 Preparation of arsenic and selenium sample solutions
6.5 Preparation of gaseous arsenic compound and gaseous
selenium compound (arsenic hydride, hydrogen selenide)
sample solutions
7 Determination of cadmium
7.1 Flame atomic absorption spectrometry
7.2 Electrothermal atomic absorption spectrometry
7.3 ICP emission spectrometry
7.4 ICP mass spectrometry
8 Determination of lead
8.1 Flame atomic absorption spectrometry
8.2 Electrothermal atomic absorption spectrometry
8.3 ICP emission spectrometry
8.4 ICP mass spectrometry
9 Determination of nickel
9.1 Dimethylglyoxime absorptiometry
9.2 Flame atomic absorption spectrometry
9.3 Electrothermal atomic absorption spectrometry
9.4 ICP emission spectrometry
9.5 ICP mass spectrometry
10 Determination of manganese
10.1 Periodic acid absorptiometry
10.2 Flame atomic absorption spectrometry
10.3 Electrothermal atomic absorption spectrometry
10.4 ICP emission spectrometry
10.5 ICP mass spectrometry
11 Determination of vanadium
11.1 N-benzoyl-N-phenylhydroxylamine absorptiometry
11.2 Flame atomic absorption spectrometry
11.3 Electrothermal atomic absorption spectrometry
11.4 ICP emission spectrometry
11.5 ICP mass spectrometry
12 Determination of chromium
12.1 Diphenylcarbazide absorptiometry
12.2 Flame atomic absorption spectrometry
12.3 Electrothermal atomic absorption spectrometry
12.4 ICP emission spectrometry
12.5 ICP mass spectrometry
13 Determination of beryllium
13.1 Flame atomic absorption spectrometry
13.2 Electrothermal atomic absorption spectrometry
13.3 ICP emission spectrometry
13.4 ICP mass spectrometry
14 Determination of arsenic
14.1 Silver diethyldithiocarbamate absorptiometry
14.2 Hydride-generation atomic absorption spectrometry
14.3 Electrothermal atomic absorption spectrometry
14.4 Hydride-generation ICP emission spectrometry
14.5 ICP mass spectrometry
15 Determination of selenium
15.1 3,3'-diaminobenzidine absorptiometry
15.2 Hydride-generation atomic absorption spectrometry
15.3 Electrothermal atomic absorption spectrometry
15.4 Diaminonaphthalene fluorophotometry
15.5 Hydride-generation ICP emission spectrometry
15.6 ICP mass spectrometry
16 Calculation
Attached table 1 Normative references
Annex (normative) Pretreatment of sample using microwave
heating pressure vessel

Abstract

Specifies the methods for determination of cadmium, lead, nickel, manganese, vanadium, chromium, beryllium, arsenic and selenium in particulate substances, and arsenic and selenium in gaseous substances among the metals which exist in the gas exhausted from a flue, chimney, or duct, due to such processes as burning of fuels or other materials, and refining, working and physicochemical-treatment of metals.

General Product Information

Published
Document Type	Standard
Status	Current
Publisher	Japanese Standards Association
Pages
ISBN
Supersedes	JIS K 0224:1983 JIS K 0223:1983 JIS K 0084:1976 JIS K 0096:1975 JIS K 0083:2006